解:设样品中H2C2O4的质量为X23.76ml氢氧化钠溶液中含氢氧化钠的物质的量=0.1024mol/L*0.02376L=0.002433024mol2NaOH + H2C2O4= Na2C2O4+2H2O 2 90.040.002433024mol XX=0.10953g样品中H2C2O4的百分含量=0.10953g/0.1140g*100%=96.08%